Universität zu Köln

Lingscheid, Yves, Paul, Mathias, Broehl, Andreas, Neudoerfl, Joerg-Martin and Giernoth, Ralf ORCID: 0000-0003-2282-6586 (2018). Determination of inter-ionic and intra-ionic interactions in a monofluorinated imidazolium ionic liquid by a combination of X-ray crystallography and NOE NMR spectroscopy. Magn. Reson. Chem., 56 (2). S. 80 - 86. HOBOKEN: WILEY. ISSN 1097-458X

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Abstract

We report the very first application of a Transient 1D H-1{F-19} NOE NMR experiment in neat ionic liquids. In comparison with classical 2D HOESY NMR spectroscopy, a substantial reduction in measurement time is gained with comparable quality and information content of the spectra. In combination with classical X-ray crystallography, we have applied this technique for the determination of inter-ionic distances (i.e. probabilities of presence) utilizing an ionic liquid containing a monofluorinated imidazolium cation. Copyright (c) 2017 John Wiley & Sons, Ltd.

Item Type:	Journal Article
Creators:	Creators Email ORCID ORCID Put Code Lingscheid, Yves UNSPECIFIED UNSPECIFIED UNSPECIFIED Paul, Mathias UNSPECIFIED UNSPECIFIED UNSPECIFIED Broehl, Andreas UNSPECIFIED UNSPECIFIED UNSPECIFIED Neudoerfl, Joerg-Martin UNSPECIFIED UNSPECIFIED UNSPECIFIED Giernoth, Ralf UNSPECIFIED orcid.org/0000-0003-2282-6586 UNSPECIFIED
URN:	urn:nbn:de:hbz:38-198319
DOI:	10.1002/mrc.4608
Journal or Publication Title:	Magn. Reson. Chem.
Volume:	56
Number:	2
Page Range:	S. 80 - 86
Date:	2018
Publisher:	WILEY
Place of Publication:	HOBOKEN
ISSN:	1097-458X
Language:	English
Faculty:	Faculty of Mathematics and Natural Sciences
Divisions:	Faculty of Mathematics and Natural Sciences > Department of Chemistry > Institute of Organic Chemistry
Subjects:	no entry
Uncontrolled Keywords:	Keywords Language INTERMOLECULAR NOES; SHORT-RANGE; LONG-RANGE; DYNAMICS; SALTS; WATER Multiple languages Chemistry, Multidisciplinary; Chemistry, Physical; Spectroscopy Multiple languages
Refereed:	Yes
URI:	http://kups.ub.uni-koeln.de/id/eprint/19831