Universität zu Köln

Renzi, Polyssena ORCID: 0000-0002-1326-8183, Kronig, Christel, Carlone, Armando ORCID: 0000-0003-2983-6445, Eroksuz, Serap, Berkessel, Albrecht ORCID: 0000-0003-0470-7428 and Bella, Marco (2014). Kinetic Resolution of Oxazinones: Rational Exploration of Chemical Space through the Design of Experiments. Chem.-Eur. J., 20 (37). S. 11768 - 11776. WEINHEIM: WILEY-V C H VERLAG GMBH. ISSN 1521-3765

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Abstract

The organocatalytic kinetic resolution of 4-substituted oxazinones has been optimised (selectivity factor S up to 98, chiral oxazinone ee values up to 99.6% (1a-g) and product ee values up to 90% (3a-g)) in a rational way by applying the Design of Experiments (DoE) approach.

Item Type:	Journal Article
Creators:	Creators Email ORCID ORCID Put Code Renzi, Polyssena UNSPECIFIED orcid.org/0000-0002-1326-8183 UNSPECIFIED Kronig, Christel UNSPECIFIED UNSPECIFIED UNSPECIFIED Carlone, Armando UNSPECIFIED orcid.org/0000-0003-2983-6445 UNSPECIFIED Eroksuz, Serap UNSPECIFIED UNSPECIFIED UNSPECIFIED Berkessel, Albrecht UNSPECIFIED orcid.org/0000-0003-0470-7428 UNSPECIFIED Bella, Marco UNSPECIFIED UNSPECIFIED UNSPECIFIED
URN:	urn:nbn:de:hbz:38-428893
DOI:	10.1002/chem.201402380
Journal or Publication Title:	Chem.-Eur. J.
Volume:	20
Number:	37
Page Range:	S. 11768 - 11776
Date:	2014
Publisher:	WILEY-V C H VERLAG GMBH
Place of Publication:	WEINHEIM
ISSN:	1521-3765
Language:	English
Faculty:	Faculty of Mathematics and Natural Sciences
Divisions:	Faculty of Mathematics and Natural Sciences > Department of Chemistry > Institute of Organic Chemistry
Subjects:	no entry
Uncontrolled Keywords:	Keywords Language MICHAEL ADDITION; ORGANOCATALYSTS; OPTIMIZATION; ALCOHOLS Multiple languages Chemistry, Multidisciplinary Multiple languages
Refereed:	Yes
URI:	http://kups.ub.uni-koeln.de/id/eprint/42889