Walbaum, Christine, Pantenburg, Ingo and Meyer, Gerd (2011). Iodine Molecules Included in the Structure of Dibenzo-24-Crown-8, (I-2)@(db24c8). Crystals, 1 (4). S. 215 - 220. BASEL: MDPI AG. ISSN 2073-4352
Full text not available from this repository.Abstract
A reaction of YI3, dibenzo-24-crown-8 and iodine in ethanol yielded, as a by-product, red single crystals of (I-2)@(db24c8). In the triclinic crystal, P-1, a = 485.0(1), b = 1203.7(3), c = 1280.4(2) pm, alpha = 64.56(2)degrees, beta = 86.82(2)degrees, gamma = 83.89(2)degrees, V = 671.1(2) x 10(6) pm(3), Z = 1, R-1= 0.0301 for 1965 reflections with I-0 > 2 sigma(I-0), iodine molecules with an I-I distance of 268.39(7) pm, slightly longer than in the gas phase, are included in a matrix of db24c8 molecules.
Item Type: | Journal Article | ||||||||||||||||
Creators: |
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URN: | urn:nbn:de:hbz:38-484764 | ||||||||||||||||
DOI: | 10.3390/cryst1040215 | ||||||||||||||||
Journal or Publication Title: | Crystals | ||||||||||||||||
Volume: | 1 | ||||||||||||||||
Number: | 4 | ||||||||||||||||
Page Range: | S. 215 - 220 | ||||||||||||||||
Date: | 2011 | ||||||||||||||||
Publisher: | MDPI AG | ||||||||||||||||
Place of Publication: | BASEL | ||||||||||||||||
ISSN: | 2073-4352 | ||||||||||||||||
Language: | English | ||||||||||||||||
Faculty: | Unspecified | ||||||||||||||||
Divisions: | Unspecified | ||||||||||||||||
Subjects: | no entry | ||||||||||||||||
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URI: | http://kups.ub.uni-koeln.de/id/eprint/48476 |
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