Universität zu Köln

Walbaum, Christine, Pantenburg, Ingo and Meyer, Gerd (2011). Iodine Molecules Included in the Structure of Dibenzo-24-Crown-8, (I-2)@(db24c8). Crystals, 1 (4). S. 215 - 220. BASEL: MDPI AG. ISSN 2073-4352

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Abstract

A reaction of YI3, dibenzo-24-crown-8 and iodine in ethanol yielded, as a by-product, red single crystals of (I-2)@(db24c8). In the triclinic crystal, P-1, a = 485.0(1), b = 1203.7(3), c = 1280.4(2) pm, alpha = 64.56(2)degrees, beta = 86.82(2)degrees, gamma = 83.89(2)degrees, V = 671.1(2) x 10(6) pm(3), Z = 1, R-1= 0.0301 for 1965 reflections with I-0 > 2 sigma(I-0), iodine molecules with an I-I distance of 268.39(7) pm, slightly longer than in the gas phase, are included in a matrix of db24c8 molecules.

Item Type:	Journal Article
Creators:	Creators Email ORCID ORCID Put Code Walbaum, Christine UNSPECIFIED UNSPECIFIED UNSPECIFIED Pantenburg, Ingo UNSPECIFIED UNSPECIFIED UNSPECIFIED Meyer, Gerd UNSPECIFIED UNSPECIFIED UNSPECIFIED
URN:	urn:nbn:de:hbz:38-484764
DOI:	10.3390/cryst1040215
Journal or Publication Title:	Crystals
Volume:	1
Number:	4
Page Range:	S. 215 - 220
Date:	2011
Publisher:	MDPI AG
Place of Publication:	BASEL
ISSN:	2073-4352
Language:	English
Faculty:	Unspecified
Divisions:	Unspecified
Subjects:	no entry
Uncontrolled Keywords:	Keywords Language Crystallography; Materials Science, Multidisciplinary Multiple languages
URI:	http://kups.ub.uni-koeln.de/id/eprint/48476